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High field liquid phase and solid state NMR

Queen Mary’s high field Nuclear Magnetic Resonance (NMR) service is equipped with a Bruker AV600 spectrometer featuring:

  • Four channels
  • Gradients - A new (long coil) 5mm H/C/N inverse triple resonance probe
  • Other solution state probes, including:
    • 5mm 1H/19F dual
    • 5mm BB 28 - 242 MHz (109Ag - 31P)
    • 8mm 13C/1H dual
    • 10mm BB 10 - 51 MHz (191Ir - 169Tm)
  • An automatic sample changer with capacity for up to 60 samples
  • Solid state capability with the following probes:
    • 4mm MAS BB 92 - 242 MHz (2H - 31P)
    • 4mm CP/MAS BB 61 - 242 MHz (15N - 31P)
    • 7mm CP/MAS BB 28 - 61 MHz (39K - 15N)
    • Variable temperature control from -120oC to 200oC
  • Software available for processing and analysing NMR data, including:
    • XwinNMR and TopSpin – Bruker's standard acquisition and processing suites
    • Aurelia – for analysis of 2-4D NMR datasets
    • Amix - for a wide variety of applications, such as metabolomics, small molecules research and mixture analysis

Find out more on the high field NMR server website.

Contact

To find out more about this service, contact our NMR Facility Manager Dr Harold Toms.

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