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High field liquid phase and solid state NMR

Queen Mary’s high field Nuclear Magnetic Resonance (NMR) service is equipped with a Bruker AV600 spectrometer featuring:

  • Four channels
  • Gradients - A new (long coil) 5mm H/C/N inverse triple resonance probe
  • Other solution state probes, including:
    • 5mm 1H/19F dual
    • 5mm BB 28 - 242 MHz (109Ag - 31P)
    • 8mm 13C/1H dual
    • 10mm BB 10 - 51 MHz (191Ir - 169Tm)
  • An automatic sample changer with capacity for up to 60 samples
  • Solid state capability with the following probes:
    • 4mm MAS BB 92 - 242 MHz (2H - 31P)
    • 4mm CP/MAS BB 61 - 242 MHz (15N - 31P)
    • 7mm CP/MAS BB 28 - 61 MHz (39K - 15N)
    • Variable temperature control from -120oC to 200oC
  • Software available for processing and analysing NMR data, including:
    • XwinNMR and TopSpin – Bruker's standard acquisition and processing suites
    • Aurelia – for analysis of 2-4D NMR datasets
    • Amix - for a wide variety of applications, such as metabolomics, small molecules research and mixture analysis

Find out more on the high field NMR server website.

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